Manufacturer of Petroleum Test Equipment since 1873

Product   

 Distillation at Atmospheric Pressure - ADU 4 (automatic)


Main Unit   

11-0542

 

ADU 4 - Automatic Distillation Unit with Fire-Extinguisher

Petroleum Products at Atmospheric Pressure: ASTM D 86 -
IP 123 - ISO 3405 (DIN 51751 - NF M07-002) - JIS K2254

With further accessories suitable for:
Industrial Aromatic Hydrocarbons: ASTM D 850
Volatile Organic Liquids: ASTM D 1078 - IP 195

Consisting of:
Heating cabinet with built-in fire-extinguisher, microprocessor controlled electric heater (1200 W), temperature probe and jack for height adjustment of flask. Condenser tube with water jacket for tempering by external thermostatic circulator. Recovery cabinet with light barrier detection.
High-grade stainless steel housing with two-color powder coating, digital display, keys and RS232 interface.

Supplied with:
1 ADUcon-software to allow a computer-supported operation
1 ADUpro-software as PC extension module with additional functions:
   - Heat-Parameter Optimizer (If necessary, this software recommends more adequate heat-
     parameters for the next test run automatically.
   - Pre-selected Temperature-Spread-Sheet (additionally to the Volume-Spread-Sheet the selection
     of nearly all temperature-values and the corresponding volume recovered is possible)
   - Support of solvent distillation acc. ASTM D 850 & D 1078
     (with a preset parameter library for different solvents)
   - Connection and simultaneous run of up to 6 ADU-units with 1 PC
     (if not enough RS232-ports available, we recommend a USB-Hub)
     Note: Each ADU-unit requires a separate ADUpro-Software installation.
1 glassware set according ASTM D 86 (Group 1-4)
   (1 flask 125 ml, 2 glass-ceramic plates with hole 1x Ø 38 & 1x Ø 50 mm)
1 PTFE-stopper 19/26 to hold the temperature probe
1 stopper to connect flask condenser tube
1 graduated cylinder 100 ml with metal base
1 drip tongue
1 cleaning coil for the condenser tube
1 test sample (300 ml bottle)
1 insulating hose set for cooler connection
1 connection set
  (data cable for cooler, 0-modem cable, RS232-adapter, USB-converter)

Power supply: 230 V, 50 Hz

 

11-0543

 

ADU 4 - Automatic Distillation Unit with Fire-Extinguisher

Like 11-0542 but:
Power supply: 115 V, 60 Hz

 



11-1542

 

ADU 4 - Automatic Distillation Unit with Dry-Point Detection & Fire-Extinguisher

Petroleum Products at Atmospheric Pressure: ASTM D 86 -
IP 123 - ISO 3405 (DIN 51751 - NF M07-002) - JIS K2254

With further accessories suitable for:
Industrial Aromatic Hydrocarbons: ASTM D 850
Volatile Organic Liquids: ASTM D 1078 - IP 195

Like 11-0542 but: A sensor for dry-point detection must be ordered separately (acc. to flask size). Further it requires external CO2 or N2 supply between 6 and 12 bar.

Power supply: 230 V, 50 Hz

 

11-1543

 

ADU 4 - Automatic Distillation Unit with Dry-Point Detection & Fire-Extinguisher

Like 11-1542 but:
Power supply: 115 V, 60 Hz

 


Options & Accessories   

11-0546

 

Glassware Set (Group 0-4)

Glassware Set (Group 0-4)

ASTM D 86 - ISO 3405 - IP 123 - JIS K2254
Consisting of:
1 flask 100 ml, neck 19/26 (group 0)
1 glass-ceramic plate with hole Ø 32 mm (group 0)
1 flask 125 ml, neck 19/26 (group 1-4)
1 glass-ceramic plate with hole Ø 38 mm (group 1-4)
1 glass-ceramic plate with hole Ø 50 mm (group 1-4)

 

11-0536

 

Glassware Set (Group 1-4)

Glassware Set (Group 1-4)

ASTM D 86 - ISO 3405 - IP 123 - JIS K2254
Consisting of:
1 flask 125 ml, neck 19/26 (group 1-4)
1 glass-ceramic plate with hole Ø 38 mm (group 1-4)
1 glass-ceramic plate with hole Ø 50 mm (group 1-4)

 

11-0524

 

Distillation Flask, 125 ml, ground socket (NS 19/26)

with thermometer immersion-mark, side pipe Ø 7 mm,
quartz glass (for temperatures above 370 °C)
(ASTM E133/B, Engler-shape)

 

11-0588

 

Dry-Point Sensor fits 100/125 ml flask

 



11-0547

 

Glassware Set (Solvents)

Glassware Set (Solvents)

ASTM D 850 - ASTM D 1078 - IP 195
Consisting of:
1 flask 200 ml, neck 19/26
1 glass-ceramic plate with hole Ø 25 mm
1 glass-ceramic plate with hole Ø 32 mm
1 glass-ceramic plate with hole Ø 38 mm
1 glass-ceramic plate with hole Ø 50 mm

 

11-0596

 

Cylinder HR, 100 ml, borosilicate glass, graduated

(complete with tube, metal base and O-rings)

 

11-0587

 

Dry-Point Sensor fits 200 ml flask

 



11-0575

 

Anti-Dazzle Screen

Anti-Dazzle Screen

(for dazzling-free dry-point observations)

 

11-0571

 

Calibration Set - ADU4 Volume-Detection

Calibration Set - Volume-Detection

Consisting of:
1 Burette (50:0.1 ml)
1 Burette-holder set

 

11-0582

 

Calibration Set - ADU4/4+ Temperature

Calibration-Set - Temperature

Consisting of:
1 Calibration-Resistor-Set
1 Thermometer IP 39C (official certified)

 

11-0590

 

Reference Liquid - Distillation of Mineral Oil Products
(Boiling Characteristics)

ASTM D 86 - ISO 3405

Initial Boiling Point: approx. 160°C,
Final Boiling Point: approx. 360°C
Data evaluated by International Industrial Round Robin Test.

Aluminum bottle / content 255 ml.

 

11-0591

 

Reference Liquid - Distillation of Gasoline (Unleaded)

ASTM D 86

Certified Value: approx. 30 °C - 184 °C, 250 ml

 

11-0593

 

Reference Liquid - Distillation of Diesel

ASTM D 86

Certified Value: approx. 163 °C to 362 °C, 250 ml

 

11-0545

 

Boiling-Stones, pack of 20 g

Boiling-Stones

against the boiling retardation
Note: Do not use with dry-point detection.

 

11-0597

 

O-Ring Set (Chemraz), solvent resistant

(used for condenser tube stopper and flask-neck)

 



25-0803

 

Computer with Monitor & Graphic-Printer

allows to connect up to 6 instruments
(detailed specifications upon request)
Power supply: 230 V, 50 Hz

 

11-0598

 

USB-Hub Device (4-ports) with power supply (EU-plug)

to connect 4 instruments by USB 2.0 to one PC USB-port, (Verified for petrotest® units)

 

11-0594

 

USB-Hub Device (4-ports) with power supply (US-plug-adapter)

 


25-0282

 

Impact Printer (mono)

Serial Printer

for single sheets & continuous paper
to record data like test results, duration of test, etc. (instead of a PC)

Supplied with: 2 data cables (9-pin 25-0304, USB 25-0918), 1 ink ribbon (black)

Technical Data:
Line spacing: 80 characters per line (10 cpi)
Page size : 257 x 364 mm (sheet), 254 x 558.8 mm (roll)
Ports: serial (9-pin), USB (1.1)
Dimensions: 37 x 28 x 16 cm (WxDxH)
Weight: 5 kg
Power supply: 220/240 V, 50/60 Hz

 

25-0283

 

Impact Printer

Like 25-0282 but:
Power supply: 110/130 V, 50/60 Hz

 



25-0240

 

Circulator (-28/+200)

Circulator F25-MA

For heating & cooling of instruments without circulation pump
and / or for tempering applications directly in the bath.

Consisting of:
Cooler with stainless steel bath.Thermostat with digital display, splash-proof keypad, integrated heater, pump, RS232-interface, over/under-temperature & low-level protection, adjustable pump-pressure, cooling control.

Supplied with: 1 bath cover, 1 drain tap

Note: Insulated hose-set is recommended.

Technical Data:
Working range: -28 to +200 °C (at +5 to +40 °C ambient temp.)
Display / Resolution: LED / 0.01 or 0.1 °C
Heater capacity: 2000 W
Cooling capacity: 260 W at +20 °C
Pump-Pressure capacity: 11-16 l/min, , 0.23-0.45 bar (3.3-6.5 psi)
Bath opening: 12 x 14 x 14 cm (WxDxH)
Safety class / Bath fluid: 3 / FL (Flammable Liquids possible)
Volume: 4.5 l
Sockets for: hose (Ø 8 / 10 mm), solenoid valve
Dimensions / Weight: 23 x 42 x 61 cm (WxDxH), 31 kg
Power supply: 230 V, 50/60 Hz, 12 A, EU-plug

 

25-0241

 

Circulator (-28/+200)

Like 25-0240 but:
Heater capacity: 1000 W
Power supply: 115 V, 60 Hz, US-plug

 


25-0242

 

Circulator (-35/+200)

Circulator

For heating & cooling of instruments without circulation pump
and / or for tempering applications directly in the bath.

Consisting of:
Cooler with stainless steel bath. Thermostat with digital display, splash-proof keypad, integrated heater, pump, RS232-interface, over/under-temperature & low-level protection, adjustable pump-pressure, cooling control.

Supplied with: 1 bath cover, 1 drain tap

Note: Insulated hose-set is recommended

Technical Data:
Working range: -35 to +200 °C (at +5 to +40 °C ambient temp.)
Display / Resolution: LED / 0.01 or 0.1 °C
Heater capacity: 2000 W
Cooling capacity: 450 W at +20 °C
Pump-Pressure capacity: 11-16 l/min, 0.23-0.45 bar (3.3-6.5 psi)
Bath opening: 18 x 12 x 15 cm (WxDxH)
Safety class / Bath fluid: 3 / FL (Flammable Liquids possible)
Volume: 8 l
Sockets for: hose (Ø 8 / 10 mm)
Dimensions / Weight: 31 x 42 x 64 cm (WxDxH), 37 kg
Power supply: 230 V, 50 Hz, 13 A, EU-plug

 

25-0243

 

Circulator (-35/+200)

Like 25-0242 but:
Heater capacity: 1000 W
Power supply: 115 V, 60 Hz, US-plug

 






Spare Parts   

11-0574

 

Spare Parts Set - ASTM D 86 (Group 1-4)

Spare Parts Set - ASTM D 86

for approx. 1 year consisting of:
10x 11-0515 (125 ml flask),
  2x 11-0554 (100 ml cylinder),
  1x 11-0558 (5 stoppers),
  1x 11-0559 (temperature probe),
  1x 11-0567 (drip tongue)

 

11-0514

 

Distillation Flask, 100 ml, ground socket (NS 19/26)

with thermometer immersion-mark, side pipe Ø 7 mm,
(ASTM E133/A, Engler-shape)

 

11-0515

 

Distillation Flask, 125 ml, ground socket (NS 19/26)

with thermometer immersion-mark, side pipe Ø 7 mm,
(ASTM E133/B, Engler-shape)

 

11-0524

 

Distillation Flask, 125 ml, ground socket (NS 19/26)

with thermometer immersion-mark, side pipe Ø 7 mm,
quartz glass (for temperatures above 370 °C)
(ASTM E133/B, Engler-shape)

 

11-0517

 

Distillation Flask, 200 ml, ground socket (NS 19/26)

with thermometer immersion-mark, side pipe Ø 7 mm,
(ASTM E133/C, Barret-shape)

 


11-0567

 

Drip Tongue

 


11-0554

 

Cylinder, 100 ml, borosilicate glass, graduated

(complete with tube, metal base and O-rings)

 

11-0596

 

Cylinder HR, 100 ml, borosilicate glass, graduated

(complete with tube, metal base and O-rings)

 

11-0555

 

Cylinder Tube, borosilicate glass, graduated

 

11-0556

 

Cylinder Metal Base, (fits 11-0555) with 3 O-rings

 

11-0595

 

Cylinder Metal Base HR (fits 11-0555)

with 3 O-rings (top one high resistant)

 


11-0557

 

O-Rings for metal base 11-0556 inside, pack of 10

 

11-0573

 

O-Rings for metal base 11-0556 outside, pack of 10

 

11-0572

 

Dismantling Device for cylinder metal base

 


11-0135

 

Support Board, center hole Ø 25 mm (1")

glass ceramics (150 x 150 x 4 mm)

 

11-0136

 

Support Board, center hole Ø 32 mm (1 ¼")

glass ceramics (150 x 150 x 4 mm)

 

11-0137

 

Support Board, center hole Ø 38 mm (1 ½")

glass ceramics (150 x 150 x 4 mm)

 

11-0138

 

Support Board, center hole Ø 50 mm (2")

glass ceramics (150 x 150 x 4 mm)

 

11-0561

 

Electric Heater Assembly, 1200 W

(incl. 1 heater rod with & 1 w/o sensor )

 

11-0039

 

Heater Rod, 600 W, 115/230 V

without temperature sensor

 

11-0579

 

Heater Rod, 600 W, 115/230 V

with integrated temperature sensor

 

11-0578

 

Heating-Temperature Sensor (NiCr-Ni)

 

11-0559

 

Sample-Temperature Probe (Pt-100)

 

11-0521

 

Stopper, PTFE (NS 19/26 / bored Ø 6 mm) with 2 O-rings

as temperature probe support

 

11-0549

 

Cleaning Coil for condenser tube

 

11-0558

 

Stopper PEEK (Ø 12 / bored Ø 6 mm), pack of 5

Stopper PEEK

with 3 O-rings, high-temperature resistant
(to connect condenser tube with distillation flask side pipe)

 

11-0584

 

O-Ring Set for stopper 11-0558

Consisting of: 1 outer- & 2 inner - O-rings

 

11-0564

 

Burette, 50:0.1 ml

 

11-0565

 

Burette-Holder

 

26-0037

 

Thermometer IP 39C

Range: -1 to +38 : 0.1 °C (officially certified)

 

25-0229

 

Hose-Set (Ø 10 mm)

insulated, 2x 2 m, incl. fittings

 
Order Guideline   

Minimum equipment:

1x ADU, 1x Test set, 1x Cooler

Spares (approx. 1 year):

1x Spare part set

Additional requirements:

CO2 / N2-supply (6 to 12 bar) for fire-extinguisher